di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

Base Information

Chemical Name:di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate
CAS No.:241485-20-1
Molecular Formula:C₅₀H₆₈N₂O₄
Molecular Weight:761.101
Hs Code.:

Synonyms:di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

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Chemical Property of di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

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Technology Process of di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

There total 10 articles about di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: di-3-pentyl (3R,αR,E)-3-N-benzyl-N-α-methylbenzylamino-dec-8-enedioate

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 241485-20-1
di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

Guidance literature:: (S)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

di-3-pentyl (3R,αR,E)-3-N-benzyl-N-α-methylbenzylamino-dec-8-enedioate; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1039/b500223k

Reference yield: 67.0%

: lithium benzyl-(R)-1-phenylethylamide

: 1,10-di(pentan-3-yl) (2E,8E)-deca-2,8-dienedioate

: 241485-20-1
di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

Guidance literature:: DOI:10.1016/S0957-4166(99)00170-6

Reference yield:

: 1,10-di(pentan-3-yl) (2E,8E)-deca-2,8-dienedioate

: 241485-20-1
di-3-pentyl (3R,αR,8S,α'S)-3,8-bis-N-benzyl-N-α-methylbenzylamino-decadioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran / 0.5 h / -78 °C

1.2: 42 percent / tetrahydrofuran / 2 h / -78 °C

2.1: n-BuLi / tetrahydrofuran / 0.5 h / -78 °C

2.2: 71 percent / tetrahydrofuran / 2 h / -78 °C

With n-butyllithium; In tetrahydrofuran;
DOI:10.1039/b500223k