C₂₂H₂₀N₂O₆

Base Information

Chemical Name:C₂₂H₂₀N₂O₆
CAS No.:1332457-18-7
Molecular Formula:C₂₂H₂₀N₂O₆
Molecular Weight:408.411
Hs Code.:

C<sub>22</sub>H<sub>20</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₂H₂₀N₂O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₀N₂O₆

Chemical Property:

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Technology Process of C₂₂H₂₀N₂O₆

There total 8 articles about C₂₂H₂₀N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1332456-99-1
1-[3-C-phenylethynyl-3-O-(2-propynyl)-β-D-ribo-pentofuranosyl]uracil

: 74-86-2,25067-58-7
acetylene

: 1332457-18-7
C₂₂H₂₀N₂O₆

Guidance literature:: With (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride; In 1,2-dichloro-ethane; at -78 - 20 ℃;
DOI:10.1016/j.tetlet.2011.06.100

Reference yield:

: 1332457-07-4
C₂₄H₂₈O₆

: 1332457-18-7
C₂₂H₂₀N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: water; acetic acid / 2 h / Reflux

2: dmap; triethylamine / dichloromethane / 1 h / 20 °C

3: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / 50 °C

4: methanol; sodium methylate / 0.33 h / 20 °C

5: (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride / 1,2-dichloro-ethane / -78 - 20 °C

With methanol; dmap; N,O-bis-(trimethylsilyl)-acetamide; (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride; trimethylsilyl trifluoromethanesulfonate; water; sodium methylate; acetic acid; triethylamine; In dichloromethane; 1,2-dichloro-ethane; acetonitrile; 4: Zemplen deacetylation;
DOI:10.1016/j.tetlet.2011.06.100

Reference yield:

: 1332457-10-9
C₂₅H₂₈O₈

: 1332457-18-7
C₂₂H₂₀N₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / 50 °C

2: methanol; sodium methylate / 0.33 h / 20 °C

3: (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride / 1,2-dichloro-ethane / -78 - 20 °C

With methanol; N,O-bis-(trimethylsilyl)-acetamide; (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride; trimethylsilyl trifluoromethanesulfonate; sodium methylate; In 1,2-dichloro-ethane; acetonitrile; 2: Zemplen deacetylation;
DOI:10.1016/j.tetlet.2011.06.100