2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

Base Information

Chemical Name:2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate
CAS No.:1528768-69-5
Molecular Formula:C₃₁H₂₅Cl₂NO₆
Molecular Weight:578.449
Hs Code.:

Synonyms:2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

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Chemical Property of 2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

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Technology Process of 2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

There total 5 articles about 2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 15307-86-5
[2-(2,6-dichloroanilino)phenyl]acetic acid

: 1402923-75-4
2-phenyl-1,3-dioxan-5-yl 4-hydroxybenzoate

: 15362-40-0
1-(2,6-dichlorophenyl)indolin-2-one

: 1528768-69-5
2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1002/jps.24665

Reference yield: 62.0%

: 15307-86-5
[2-(2,6-dichloroanilino)phenyl]acetic acid

: 1402923-75-4
2-phenyl-1,3-dioxan-5-yl 4-hydroxybenzoate

: 1528768-69-5
2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 18h;

Reference yield:

: 99-96-7
4-hydroxy-benzoic acid

: 1528768-69-5
2-phenyl-1,3-dioxan-5-yl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / toluene; tetrahydrofuran / 16 h / 0 - 20 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 72 h / 20 °C

3: ammonium acetate; water / methanol / 16 h / 20 °C

4: dicyclohexyl-carbodiimide; dmap / dichloromethane / 18 h / 0 - 20 °C

With pyridine; dmap; ammonium acetate; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; toluene;