2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Base Information

Chemical Name:2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine
CAS No.:1334291-40-5
Molecular Formula:C₄₀H₆₃NO₂
Molecular Weight:589.946
Hs Code.:

Synonyms:2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Suppliers and Price of 2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

There total 7 articles about 2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₇NO₄

: 60902-45-6
nonyltriphenylphosphonium bromide

: 1334291-39-2
2-(5-(4-methoxybenzyloxy)pentyl)-4,6-dimethyl-3,5-di((Z)-dec-1-enyl)pyridine

: 1334291-40-5
2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -70 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.07.058

Reference yield:

: 1334291-36-9
2-(5-(4-methoxybenzyloxy)pent-1-ynyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

: 1334291-39-2
2-(5-(4-methoxybenzyloxy)pentyl)-4,6-dimethyl-3,5-di((Z)-dec-1-enyl)pyridine

: 1334291-40-5
2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 5%-palladium/activated carbon; hydrogen / methanol / 6 h / 20 °C / 2999.54 Torr

2: diisobutylaluminium hydride / toluene / 0.83 h / -15 - 0 °C / Inert atmosphere

3: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / -70 - 20 °C / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; diisobutylaluminium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; toluene; 3: Wittig reaction;
DOI:10.1016/j.bmcl.2011.07.058

Reference yield:

: 1334291-37-0
2-(5-(4-methoxybenzyloxy)pentyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

: 1334291-39-2
2-(5-(4-methoxybenzyloxy)pentyl)-4,6-dimethyl-3,5-di((Z)-dec-1-enyl)pyridine

: 1334291-40-5
2-(5-(4-methoxybenzyloxy)pentyl)-3,5-di((E)-dec-1-enyl)-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / toluene / 0.83 h / -15 - 0 °C / Inert atmosphere

2: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / -70 - 20 °C / Inert atmosphere

With diisobutylaluminium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 2: Wittig reaction;
DOI:10.1016/j.bmcl.2011.07.058