(E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Base Information

Chemical Name:(E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene
CAS No.:121887-53-4
Molecular Formula:C₃₀H₂₁F₇O₃S
Molecular Weight:594.55
Hs Code.:

Synonyms:(E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

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Chemical Property of (E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

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Technology Process of (E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

There total 6 articles about (E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 121887-49-8
(E)-1-<4-(methylthio)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

: 121887-53-4
(E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Guidance literature:: With peroxylaurinoic acid; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jm00132a006

Reference yield:

: 104-95-0
(4-bromophenyl)thioanisole

: 121887-53-4
(E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg, Br(CH₂)2Br / 1) Et₂O, reflux, 2) Et₂O, reflux, 12 h

2: conc. H₂SO₄ / ethanol / 1 h / Ambient temperature

3: 73 percent / pyridine hydrochloride / 2 h / 200 °C

4: 4N>HSO₄, 1 M NaOH / CH₂Cl₂ / 1 h / Ambient temperature

5: 75 percent / peroxylauric acid / CH₂Cl₂ / 2 h / Ambient temperature

With sodium hydroxide; peroxylaurinoic acid; sulfuric acid; tetra(n-butyl)ammonium hydrogensulfate; pyridine hydrochloride; magnesium; ethylene dibromide; In ethanol; dichloromethane;
DOI:10.1021/jm00132a006

Reference yield:

: 78423-10-6
1-(4-methoxyphenyl)-2-phenylbutan-1-one

: 121887-53-4
(E)-1-<4-(methylsulfonyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg, Br(CH₂)2Br / 1) Et₂O, reflux, 2) Et₂O, reflux, 12 h

2: conc. H₂SO₄ / ethanol / 1 h / Ambient temperature

3: 73 percent / pyridine hydrochloride / 2 h / 200 °C

4: 4N>HSO₄, 1 M NaOH / CH₂Cl₂ / 1 h / Ambient temperature

5: 75 percent / peroxylauric acid / CH₂Cl₂ / 2 h / Ambient temperature

With sodium hydroxide; peroxylaurinoic acid; sulfuric acid; tetra(n-butyl)ammonium hydrogensulfate; pyridine hydrochloride; magnesium; ethylene dibromide; In ethanol; dichloromethane;
DOI:10.1021/jm00132a006