C₁₃H₂₀O₄

Base Information

Chemical Name:C₁₃H₂₀O₄
CAS No.:930803-44-4
Molecular Formula:C₁₃H₂₀O₄
Molecular Weight:240.299
Hs Code.:

C<sub>13</sub>H<sub>20</sub>O<sub>4</sub>

Synonyms:C₁₃H₂₀O₄

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Chemical Property of C₁₃H₂₀O₄

Chemical Property:

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Technology Process of C₁₃H₂₀O₄

There total 1 articles about C₁₃H₂₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 930803-45-5
C₆₆H₁₁₅O₁₃Si₂N

: 930803-39-7
C₅₁H₉₃O₁₁Si₂N

: 930803-44-4
C₁₃H₂₀O₄

: 1156545-80-0
C₁₅H₂₂O₄

: 1156545-79-7
C₅₃H₉₅NO₁₁Si₂

Guidance literature:: C₆₆H₁₁₅O₁₃Si₂N; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200801656

Reference yield:

: 930803-44-4
C₁₃H₂₀O₄

: 53123-88-9
sirolimus

Guidance literature:: Multi-step reaction with 14 steps

1.1: CrCl₂ / tetrahydrofuran; dioxane / 0 °C

2.1: N-methylpyrrolidinone; [Pd{P(2-furyl)3}2Cl₂]; hexamethyltin / 20 °C

2.2: [Pd{P(2-furyl)3}2Cl₂]; N-methylpyrrolidinone / 20 °C

3.1: 81 percent / LiAlH(OtBu)3 / tetrahydrofuran / -10 °C

4.1: 81 percent / 4-pyrrolidinopyridine / CH₂Cl₂

5.1: 89 percent / lithium hydroxide / H₂O; tetrahydrofuran / 0 °C

6.1: 88 percent / 2,6-lutidine / CH₂Cl₂ / -20 - 20 °C

7.1: 66 percent / 2,6-lutidine / CH₂Cl₂ / -20 °C

8.1: 88 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 0 - 20 °C

9.1: 81 percent / potassium carbonate / dimethylformamide / 20 °C

10.1: 78 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 - -20 °C

11.1: 80 percent / dimedone / [Pd(PPh₃)4] / tetrahydrofuran / 20 °C

12.1: PhI(OAc)2 / acetonitrile; H₂O / 0 °C

13.1: 2,9-dimethyl-1,10-phenanthroline; pyridine / CH₂Cl₂ / 20 °C

14.1: 61 percent / pyridine*HF / tetrahydrofuran / 50 °C

With pyridine; 2,6-dimethylpyridine; 1-methyl-pyrrolidin-2-one; chromium dichloride; dmap; lithium hydroxide; 2.9-dimethyl-1,10-phenanthroline; [bis(acetoxy)iodo]benzene; hexamethyldistannane; potassium carbonate; dimedone; 4-pyrrolidin-1-ylpyridine; pyridine hydrogenfluoride; lithium tri-t-butoxyaluminum hydride; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-44-4
C₁₃H₂₀O₄

: 930803-45-5
C₆₆H₁₁₅O₁₃Si₂N

Guidance literature:: Multi-step reaction with 2 steps

1.1: CrCl₂ / tetrahydrofuran; dioxane / 0 °C

2.1: N-methylpyrrolidinone; [Pd{P(2-furyl)3}2Cl₂]; hexamethyltin / 20 °C

2.2: [Pd{P(2-furyl)3}2Cl₂]; N-methylpyrrolidinone / 20 °C

With 1-methyl-pyrrolidin-2-one; chromium dichloride; hexamethyldistannane; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/anie.200604053