3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

Base Information

Chemical Name:3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran
CAS No.:1338381-15-9
Molecular Formula:C₃₇H₃₂O₃
Molecular Weight:524.659
Hs Code.:

Synonyms:3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

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Chemical Property of 3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

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Technology Process of 3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

There total 4 articles about 3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1338381-00-2
4-(3-(2-iodo-6-methoxy-4-((4-methylbenzyloxy)methyl)phenoxy)-1-phenylprop-1-enyl)biphenyl

: 1338381-15-9
3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

Guidance literature:: With 1,10-Phenanthroline; potassium tert-butylate; In 1,3,5-trimethyl-benzene; at 160 ℃; for 2h;
DOI:10.1039/c1cc14297f

Reference yield:

: 303111-05-9
4-(3-bromo-1-phenyl-prop-1-enyl)-biphenyl

: 1338381-15-9
3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: 1,10-Phenanthroline; potassium tert-butylate / 1,3,5-trimethyl-benzene / 2 h / 160 °C

With 1,10-Phenanthroline; potassium tert-butylate; potassium carbonate; In N,N-dimethyl-formamide; 1,3,5-trimethyl-benzene; 2: Heck reaction;
DOI:10.1039/c1cc14297f

Reference yield:

: 303110-91-0
3-phenyl-3-(biphenyl-4-yl)-prop-2-en-1-ol

: 1338381-15-9
3-(biphenyl-4-yl(phenyl)methyl)-7-methoxy-5-((4-methylbenzyloxy)methyl)benzofuran

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; triphenylphosphine / dichloromethane / 0.25 h / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: 1,10-Phenanthroline; potassium tert-butylate / 1,3,5-trimethyl-benzene / 2 h / 160 °C

With 1,10-Phenanthroline; potassium tert-butylate; bromine; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; 1,3,5-trimethyl-benzene; 3: Heck reaction;
DOI:10.1039/c1cc14297f