Technology Process of C47H63F3O9
There total 11 articles about C47H63F3O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 25 ℃;
for 2h;
DOI:10.1021/ol201426c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C
2: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 0 - 25 °C
3: diisobutylaluminium hydride / toluene / 1 h / -20 °C
4: dmap; triethylamine / dichloromethane / 2 h / 25 °C
With
dmap; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; triethylamine; tetramethylammonium triacetoxyborohydride;
In
dichloromethane; acetic acid; toluene; acetonitrile;
DOI:10.1021/ol201426c
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C
1.2: 18 h / -78 - -20 °C
2.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C
3.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 0 - 25 °C
4.1: diisobutylaluminium hydride / toluene / 1 h / -20 °C
5.1: dmap; triethylamine / dichloromethane / 2 h / 25 °C
With
dmap; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; triethylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride;
In
diethyl ether; dichloromethane; acetic acid; toluene; acetonitrile;
1.2: Aldol condensation;
DOI:10.1021/ol201426c
