methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate

Base Information

• Chemical Name: methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate
• CAS No.: 1022160-14-0
• Molecular Formula: C₄₂H₄₉N₃O₈
• Molecular Weight: 723.866

Synonyms:methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate

Chemical Property of methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate

Chemical Property:

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Technology Process of methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate

There total 1 articles about methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C23H28N2O6 (1020109-30-1) + (2,3-dibenzyloxybenzoyl)aminohexanoic acid (1022160-13-9) → methyl N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate (1022160-14-0)

Guidance literature:

C₂₃H₂₈N₂O₆; With hydrogen bromide; In dichloromethane; acetic acid; at 20 ℃; for 0.5h;

(2,3-dibenzyloxybenzoyl)aminohexanoic acid; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 17h; Further stages.;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 92.0%

methyl N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate (1022160-14-0) → N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine (1022160-15-1)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

upstream raw materials:

C₂₃H₂₈N₂O₆

(2,3-dibenzyloxybenzoyl)aminohexanoic acid

Downstream raw materials:

N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

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