6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione

Base Information

• Chemical Name: 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione
• CAS No.: 181763-50-8
• Molecular Formula: C₁₈H₁₅ClN₂OS
• Molecular Weight: 342.849

Synonyms:6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione

Chemical Property of 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione

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Technology Process of 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione

There total 1 articles about 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

thiourea (17356-08-0) + 3-(4'-chloro)phenyl-1-(2'-methoxy-4'-methyl)phenyl-2-propen-1-one → 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione (181763-50-8)

Guidance literature:

With sodium ethanolate; In ethanol; for 3h; Heating;

Reference yield: 87.0%

β-(4-phenylbenzoyl)acrylic acid (71149-96-7,34682-12-7) + 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione (181763-50-8) → 4-Biphenyl-4-yl-2-[4-(4-chloro-phenyl)-6-(2-methoxy-4-methyl-phenyl)-pyrimidin-2-ylsulfanyl]-4-oxo-butyric acid (181763-71-3)

Guidance literature:

With piperidine; In benzene; for 6h; Heating;

Reference yield: 86.0%

4-(p-methylphenyl)-4-oxo-2-butenoic acid (20972-36-5,35513-41-8,24849-45-4) + 6-(4-Chloro-phenyl)-4-(2-methoxy-4-methyl-phenyl)-1H-pyrimidine-2-thione (181763-50-8) → 2-[4-(4-Chloro-phenyl)-6-(2-methoxy-4-methyl-phenyl)-pyrimidin-2-ylsulfanyl]-4-oxo-4-p-tolyl-butyric acid (181763-70-2)

Guidance literature:

With piperidine; In benzene; for 6h; Heating;

upstream raw materials:

thiourea

Downstream raw materials:

2-[4-(4-Chloro-phenyl)-6-(2-methoxy-4-methyl-phenyl)-pyrimidin-2-ylsulfanyl]-4-oxo-4-phenyl-butyric acid

2-[4-(4-Chloro-phenyl)-6-(2-methoxy-4-methyl-phenyl)-pyrimidin-2-ylsulfanyl]-4-oxo-4-p-tolyl-butyric acid

4-Biphenyl-4-yl-2-[4-(4-chloro-phenyl)-6-(2-methoxy-4-methyl-phenyl)-pyrimidin-2-ylsulfanyl]-4-oxo-butyric acid

5-Biphenyl-4-yl-3-[4-(4-chloro-phenyl)-6-(2-methoxy-4-methyl-phenyl)-pyrimidin-2-ylsulfanyl]-3H-furan-2-one

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