2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

Base Information

Chemical Name:2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide
CAS No.:666263-06-5
Molecular Formula:C₂₀H₂₂ClF₃N₄O
Molecular Weight:426.869
Hs Code.:

Synonyms:2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

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Chemical Property of 2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

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Technology Process of 2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

There total 3 articles about 2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 666262-20-0
2-chloro-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

: 615-65-6
2-chloro-4-methyl-benzenamine

: 666263-06-5
2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

Guidance literature:: In 1,4-dioxane; for 24h; Heating / reflux;

Reference yield:

: 3218-02-8
cyclohexylmethylamine

: 666263-06-5
2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / -40 °C

2: 1,4-dioxane / 24 h / Heating / reflux

With triethylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

: 154934-99-3
2-chloro-4-(trifluoromethyl)pyrimidine-5-carbonyl chloride

: 666263-06-5
2-(2-chloro-4-methyl-phenylamino)-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / -40 °C

2: 1,4-dioxane / 24 h / Heating / reflux

With triethylamine; In 1,4-dioxane; dichloromethane;