Technology Process of C24H40O4S
There total 2 articles about C24H40O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium triethylborohydride / tetrahydrofuran / 0 °C / Inert atmosphere
2: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere
With
dmap; lithium triethylborohydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201402221
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / tert-butyl alcohol / Inert atmosphere
2: lithium triethylborohydride / tetrahydrofuran / 0 °C / Inert atmosphere
3: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere
With
dmap; lithium triethylborohydride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; tert-butyl alcohol;
DOI:10.1002/ejoc.201402221
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium iodide / N,N-dimethyl-formamide; acetone / 1.5 h / Inert atmosphere; Reflux
1.2: 1 h / 0 °C / Inert atmosphere
2.1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 25 °C / Inert atmosphere
3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; tert-butyl alcohol / tetrahydrofuran / 25 °C / Inert atmosphere
4.1: sodium periodate; water / methanol / 2 h / 0 °C / Inert atmosphere
5.1: water; sodium hydroxide / dichloromethane / 25 °C / Inert atmosphere
6.1: sodium azide; acetic acid / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere
7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 65 °C / Inert atmosphere
7.2: 0 °C / Inert atmosphere
With
1H-imidazole; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; sodium azide; water; acetic acid; 4-methylmorpholine N-oxide; potassium iodide; sodium hydroxide; tert-butyl alcohol;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
3.1: |Upjohn Dihydroxylation;
DOI:10.1002/ejoc.201402221