N-<4-prop-2-ynylamino>benzoyl>glycine

Base Information

Chemical Name:N-<4-prop-2-ynylamino>benzoyl>glycine
CAS No.:101248-34-4
Molecular Formula:C₂₁H₁₉N₅O₄
Molecular Weight:405.413
Hs Code.:

N-<4-<N-<(2-amino-4-hydroxy-6-quinazolinyl)methyl>prop-2-ynylamino>benzoyl>glycine

Synonyms:N-<4-prop-2-ynylamino>benzoyl>glycine

Suppliers and Price of N-<4-prop-2-ynylamino>benzoyl>glycine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-prop-2-ynylamino>benzoyl>glycine

Chemical Property:

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Technology Process of N-<4-prop-2-ynylamino>benzoyl>glycine

There total 4 articles about N-<4-prop-2-ynylamino>benzoyl>glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 101248-41-3
methyl N-<4-prop-2-ynylamino>benzoyl>glycinate

: 101248-34-4
N-<4-prop-2-ynylamino>benzoyl>glycine

Guidance literature:: With sodium hydroxide; In ethanol; at 25 ℃; for 4h;
DOI:10.1021/jm00156a033

Reference yield:

: 61-78-9
p-Aminohippuric acid

: 101248-34-4
N-<4-prop-2-ynylamino>benzoyl>glycine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / SOCl₂ / 22 h / -10 - 20 °C

2: 50.5 percent / K₂CO₃ / dimethylformamide; toluene / 3 h / 110 °C

3: 38 percent / CaCO₃ / various solvent(s) / 72 h

4: 77 percent / 1N NaOH / ethanol / 4 h / 25 °C

With sodium hydroxide; thionyl chloride; potassium carbonate; calcium carbonate; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00156a033

Reference yield:

: 101248-39-9
methyl N-<4-(prop-2-ynylamino)benzoyl>glycinate

: 101248-34-4
N-<4-prop-2-ynylamino>benzoyl>glycine

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / CaCO₃ / various solvent(s) / 72 h

2: 77 percent / 1N NaOH / ethanol / 4 h / 25 °C

With sodium hydroxide; calcium carbonate; In ethanol;
DOI:10.1021/jm00156a033