Technology Process of C36H44O6
There total 4 articles about C36H44O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid;
In
tetrahydrofuran;
for 1h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tet.2014.02.082
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere
2.2: 3 h / 20 °C / Reflux; Inert atmosphere
3.1: hydrogenchloride / methanol; tetrahydrofuran; water / 15 h / 20 °C
4.1: diethylazodicarboxylate; triphenylphosphine; 4-nitro-benzoic acid / tetrahydrofuran / 1 h / Inert atmosphere; Reflux
With
hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid;
In
tetrahydrofuran; methanol; water; acetone; mineral oil;
DOI:10.1016/j.tet.2014.02.082
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / methanol; tetrahydrofuran; water / 15 h / 20 °C
2: diethylazodicarboxylate; triphenylphosphine; 4-nitro-benzoic acid / tetrahydrofuran / 1 h / Inert atmosphere; Reflux
With
hydrogenchloride; triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.tet.2014.02.082
