L-Proline, 4-(1-methylethenyl)-, cis- (9CI)

Base Information

Chemical Name:L-Proline, 4-(1-methylethenyl)-, cis- (9CI)
CAS No.:111466-56-9
Molecular Formula:C₈H₁₃NO₂
Molecular Weight:155.197
Hs Code.:
Mol file:111466-56-9.mol

Synonyms:L-Proline, 4-(1-methylethenyl)-, cis- (9CI)

Suppliers and Price of L-Proline, 4-(1-methylethenyl)-, cis- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 5 raw suppliers

Chemical Property of L-Proline, 4-(1-methylethenyl)-, cis- (9CI)

Chemical Property:

Boiling Point:291.2±40.0 °C(Predicted)
PKA:2.26±0.40(Predicted)
PSA：0.00000
Density:1.088±0.06 g/cm3(Predicted)
LogP:0.00000

Purity/Quality:: 99% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of L-Proline, 4-(1-methylethenyl)-, cis- (9CI)

There total 6 articles about L-Proline, 4-(1-methylethenyl)-, cis- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100055-72-9
1-acetyl-4-isopropenyl-pyrrolidine-2-carboxylic acid methyl ester

: 98426-30-3,111466-56-9,150821-48-0
4-isopropenyl-pyrrolidine-2-carboxylic acid

Guidance literature:: With potassium hydroxide;

Reference yield:

: 98425-70-8
2-(β-ethoxy-isopropyl)-acrylonitrile

: 98426-30-3,111466-56-9,150821-48-0
4-isopropenyl-pyrrolidine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sodium ethylate; ethanol

2: Raney nickel; ethanol / 85 °C / 62518.2 Torr / Hydrogenation.Behandeln des erhaltenen 5-<β-Aethoxy-isopropyl>-2-oxo-piperidin-3-carbonsaeure-aethylesters C13H23NO4 mit SO2Cl2 in CHCl3

3: aqueous HCl / Behandeln des Reaktionsprodukts mit wss. NaOH, mit Acetanhydrid und Essigsaeure in Methanol mit Diazomethan in Aether

4: aqueous HBr / Behandeln des Reaktionsprodukts mit Acetanhydrid und Behandeln des Reaktionsprodukts in Methanol mit Diazomethan in Aether

5: aqueous KOH

With hydrogenchloride; potassium hydroxide; ethanol; hydrogen bromide; sodium ethanolate; nickel;

Reference yield:

: 99189-55-6
4-ethoxy-2-cyano-3-methyl-butyric acid ethyl ester

: 98426-30-3,111466-56-9,150821-48-0
4-isopropenyl-pyrrolidine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: aqueous NaOH-solution / Erwaermen der erhaltenen Saeure mit wss.Formaldehyd-Loesung und wenig Diaethylamin-hydrochlorid

2: sodium ethylate; ethanol

3: Raney nickel; ethanol / 85 °C / 62518.2 Torr / Hydrogenation.Behandeln des erhaltenen 5-<β-Aethoxy-isopropyl>-2-oxo-piperidin-3-carbonsaeure-aethylesters C13H23NO4 mit SO2Cl2 in CHCl3

4: aqueous HCl / Behandeln des Reaktionsprodukts mit wss. NaOH, mit Acetanhydrid und Essigsaeure in Methanol mit Diazomethan in Aether

5: aqueous HBr / Behandeln des Reaktionsprodukts mit Acetanhydrid und Behandeln des Reaktionsprodukts in Methanol mit Diazomethan in Aether

6: aqueous KOH

With hydrogenchloride; potassium hydroxide; sodium hydroxide; ethanol; hydrogen bromide; sodium ethanolate; nickel;