Technology Process of 4,10,19-tribenzyl-4,10,19-triaza-1,7,13,16-tetraoxacycloheneicosane
There total 5 articles about 4,10,19-tribenzyl-4,10,19-triaza-1,7,13,16-tetraoxacycloheneicosane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; sodium iodide;
In
acetonitrile;
for 24h;
Heating;
DOI:10.1021/jo00278a016
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 55 percent / sodium carbonate, sodium iodide / acetonitrile / 48 h / Heating
2: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating
3: 49 percent / potassium carbonate, sodium iodide / acetonitrile / 24 h / Heating
With
lithium aluminium tetrahydride; sodium carbonate; potassium carbonate; sodium iodide;
In
tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00278a016
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 65 percent / SOCl2 / CHCl3 / 1.) room temp., 1 h, 2.) reflux, 4 h
2: 55 percent / sodium carbonate, sodium iodide / acetonitrile / 48 h / Heating
3: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating
4: 49 percent / potassium carbonate, sodium iodide / acetonitrile / 24 h / Heating
With
lithium aluminium tetrahydride; thionyl chloride; sodium carbonate; potassium carbonate; sodium iodide;
In
tetrahydrofuran; chloroform; acetonitrile;
DOI:10.1021/jo00278a016
