(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

Base Information

Chemical Name:(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane
CAS No.:136693-86-2
Molecular Formula:C₂₄H₃₄N₂O₂
Molecular Weight:382.546
Hs Code.:

Synonyms:(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

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Chemical Property of (2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

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Technology Process of (2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

There total 3 articles about (2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 136778-89-7
(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-(acetylamino)azetidine

: 136693-86-2
(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃; for 20h;
DOI:10.1021/jo00018a012

Reference yield:

: 136778-88-6
(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

: 136693-86-2
(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / CHCl₃ / Ambient temperature

2: 100 percent / H₂ / 10percent Pd-C / methanol / 20 h / 25 °C

With pyridine; hydrogen; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jo00018a012

Reference yield:

: 82101-54-0
1-<(S)-1-(benzyloxy)-4-methylpent-2-yl>-(3S,4R)-3-azido-4-phenylazetidin-2-one

: 136693-86-2
(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / monochlorohydroalane / diethyl ether / 4 h / 34 °C

2: 100 percent / pyridine / CHCl₃ / Ambient temperature

3: 100 percent / H₂ / 10percent Pd-C / methanol / 20 h / 25 °C

With pyridine; hydrogen; chlorohydroalane; palladium on activated charcoal; In methanol; diethyl ether; chloroform;
DOI:10.1021/jo00018a012