dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

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Chemical Name:dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester
CAS No.:864364-96-5
Molecular Formula:C₃₇H₄₀ClNO₃S₂
Molecular Weight:646.314
Hs Code.:

dithiocarbonic acid <i>S</i>-{[<i>tert</i>-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester <i>O</i>-(2,2-dimethyl-propyl) ester

Synonyms:dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

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Chemical Property of dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

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Technology Process of dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

There total 5 articles about dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 864365-15-1
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-hydroxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

: 76-83-5
trityl chloride

: 864364-96-5
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ol051568l

Reference yield:

: 403478-26-2
4-(tert-butyl-dimethyl-silanyloxy)-2-chloro-phenylamine

: 864364-96-5
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: BF₃*OEt₂ / cyclohexane / 20 °C

2: 79 percent / N,N-dimethylaniline / CH₂Cl₂ / 20 °C

3: 86 percent / dimethylformamide / 3 h / 50 °C

4: 78 percent / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 3 h / 20 °C

With dmap; boron trifluoride diethyl etherate; N,N-dimethyl-aniline; triethylamine; In dichloromethane; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/ol051568l

Reference yield:

: 864365-13-9
tert-butyl-[4-(tert-butyl-dimethyl-silanyloxy)-2-chloro-phenyl]-amine

: 864364-96-5
dithiocarbonic acid S-{[tert-butyl-(2-chloro-4-trityloxy-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / N,N-dimethylaniline / CH₂Cl₂ / 20 °C

2: 86 percent / dimethylformamide / 3 h / 50 °C

3: 78 percent / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 3 h / 20 °C

With dmap; N,N-dimethyl-aniline; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol051568l