methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

Base Information

Chemical Name:methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside
CAS No.:1401914-55-3
Molecular Formula:C₂₁H₂₅N₃O₇S
Molecular Weight:463.511
Hs Code.:

Synonyms:methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

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Technology Process of methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

There total 4 articles about methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1401914-44-0
methyl 5-azido-3-O-benzyl-5-deoxy-α-L-idofuranosides

: 98-59-9
p-toluenesulfonyl chloride

: 1401914-55-3
methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201200110

Reference yield:

: 888954-89-0
[2-azido-2-(6-benzyloxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethoxy]-tert-butyl dimethylsilane

: 1401914-55-3
methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / 1 h / 50 °C / Inert atmosphere

2: 2,4,6-trimethyl-pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; acetyl chloride; In dichloromethane;
DOI:10.1002/chem.201200110

Reference yield:

: 763122-30-1
5-azido-6-O-tert-butyldimethylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-idofuranose

: 1401914-55-3
methyl-5-azido-3-O-benzyl-5-deoxy-6-O-p-toluenesulfonyl-α-L-idofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2: acetyl chloride / 1 h / 50 °C / Inert atmosphere

3: 2,4,6-trimethyl-pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; sodium hydride; acetyl chloride; In dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/chem.201200110