N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Base Information

Chemical Name:N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine
CAS No.:133765-70-5
Molecular Formula:C₂₄H₃₈N₄O₇
Molecular Weight:494.588
Hs Code.:

N<sup>1</sup>-<(3-nitrobenzen-1-yl)carbonyl>-N<sup>4</sup>,N<sup>8</sup>-bis(tert-butoxycarbonyl)spermidine

Synonyms:N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Suppliers and Price of N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

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Technology Process of N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

There total 1 articles about N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 68076-39-1
N₁,N₅-di-boc-spermidine

: 121-90-4
m-nitrobenzoic acid chloride

: 133765-70-5
N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Guidance literature:: With pyridine; In acetonitrile; for 3h; Ambient temperature;
DOI:10.1016/0223-5234(91)90058-U

Reference yield: 96.0%

: 133765-70-5
N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

: 133765-71-6
N¹-<(3-aminobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4h; under 760 Torr; Ambient temperature;
DOI:10.1016/0223-5234(91)90058-U

Reference yield:

: 133765-70-5
N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

: 133765-73-8
N¹-<<3-(3-aminobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

2: 92 percent / pyridine / acetonitrile / 1 h / Ambient temperature

3: 95 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/0223-5234(91)90058-U