1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI)

Base Information

Chemical Name:1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI)
CAS No.:111197-34-3
Molecular Formula:C₈H₁₂N₂O
Molecular Weight:152.196
Hs Code.:
Mol file:111197-34-3.mol

Synonyms:1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI);15,6-DIMETHYL-,4-DIAZABICYCLO[4.2.0]OCT-4-EN-8-ONE

Suppliers and Price of 1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI)

Chemical Property:

PSA：32.67000
LogP:-0.17460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI)

There total 2 articles about 1,4-Diazabicyclo[4.2.0]oct-4-en-8-one,5,6-dimethyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20012-94-6
4-methyl-4-vinylazetidin-2-one

: 111197-34-3
5,6-Dimethyl-1,4-diaza-bicyclo[4.2.0]oct-4-en-8-one

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / Bu₄N⁺Br^-

2: polymeric azide reagent / Ambient temperature

3: benzene / 14 h / Heating; method for fused ring β-lactam preparation

4: silica gel

With potassium hydroxide; polymeric azide reagent; silica gel; tetrabutylammomium bromide; In benzene;
DOI:10.1016/S0040-4039(00)95659-4