2,3,5,6-tetrafluoro-4-nitrobenzenethiol

Base Information

• Chemical Name: 2,3,5,6-tetrafluoro-4-nitrobenzenethiol
• CAS No.: 107954-62-1
• Molecular Formula: C₆HF₄NO₂S
• Molecular Weight: 227.139
• Mol file: 107954-62-1.mol

Synonyms:2,3,5,6-tetrafluoro-4-nitrobenzenethiol

Chemical Property of 2,3,5,6-tetrafluoro-4-nitrobenzenethiol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,5,6-tetrafluoro-4-nitrobenzenethiol

There total 1 articles about 2,3,5,6-tetrafluoro-4-nitrobenzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2,3,5,6-tetrafluoro-4-nitrobenzenethiol (107954-62-1)

Guidance literature:

Pentafluornitrobenzol, Dimethylformamid, Pentafluorthiophenol (Yakobson et al., Zh. Obshch. Khim. 37 (6) <1967> 1289);

DOI:10.1016/S0040-4039(01)96895-9

Reference yield: 90.0%

2,3,5,6-tetrafluoro-4-nitrobenzenethiol (107954-62-1) → 2,3,5,6-tetrafluoro-4-nitrophenylsulfenyl chloride (530102-84-2)

Guidance literature:

With chlorine; In tetrachloromethane; at 20 ℃;

DOI:10.1002/ejic.200390016

Reference yield:

2,3,5,6-tetrafluoro-4-nitrobenzenethiol (107954-62-1) → 2,3,5,6-tetrafluoro-4-nitroaniline (776-16-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / Cl₂ / CCl₄ / 20 °C

2: CH₂Cl₂ / 16 h / 20 °C

3: 74 percent / CsF / acetonitrile / 0.5 h / Heating

With chlorine; cesium fluoride; In tetrachloromethane; dichloromethane; acetonitrile;

DOI:10.1002/ejic.200390016

Downstream raw materials:

2,3,5,6-tetrafluoro-4-nitrophenylsulfenyl chloride

2,3,5,6-tetrafluoro-4-nitroaniline

1-(4-nitro-2,3,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene