12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene

Base Information

• Chemical Name: 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene
• CAS No.: 1426819-69-3
• Molecular Formula: C₃₆H₃₃N₇O₁₃S₃
• Molecular Weight: 867.895

Synonyms:12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene

Chemical Property of 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene

Chemical Property:

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Technology Process of 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene

There total 6 articles about 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(benzyloxy)-2,6-bis(chloromethyl)pyridine (171000-40-1) + N1,N3,N5-tris(2-nitrobenzenesulfonyl)-1,5-diamino-3-azapentane (210303-79-0) → 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-(15),11,13-triene (1426819-69-3)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 28h; Inert atmosphere;

DOI:10.1039/c2cc36808k

Reference yield:

4-(benzyloxy)-2,6-bis(hydroxymethyl)pyridine (115148-04-4) → 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-(15),11,13-triene (1426819-69-3)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / 4 h / 60 °C

2: sodium carbonate / N,N-dimethyl-formamide / 28 h / 100 °C / Inert atmosphere

With thionyl chloride; sodium carbonate; In N,N-dimethyl-formamide;

DOI:10.1039/c2cc36808k

Reference yield:

2-Nitrobenzenesulfonyl chloride (1694-92-4) → 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-(15),11,13-triene (1426819-69-3)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 h / 20 °C / Inert atmosphere

2: sodium carbonate / N,N-dimethyl-formamide / 28 h / 100 °C / Inert atmosphere

With sodium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c2cc36808k

upstream raw materials:

4-(benzyloxy)-2,6-bis(hydroxymethyl)pyridine

4-(benzyloxy)-2,6-bis(chloromethyl)pyridine

N¹,N³,N⁵-tris(2-nitrobenzenesulfonyl)-1,5-diamino-3-azapentane

2-Nitrobenzenesulfonyl chloride

Downstream raw materials:

12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride

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