7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane

Base Information

Chemical Name:7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane
CAS No.:58688-38-3
Molecular Formula:C₁₂H₂₆N₂O₃
Molecular Weight:246.35
Hs Code.:

Synonyms:7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane

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Chemical Property of 7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane

Chemical Property:

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Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of 7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane

There total 2 articles about 7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3065-46-1
1,2-bis-(2-dimethylamino-ethoxy)-ethane

: 58688-38-3
7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / acetonitrile / 20 h / 25 °C / 8250660 Torr

2: 77 percent / triphenylphosphine / dimethylformamide / Heating

With triphenylphosphine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c39890000184

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 58688-38-3
7,13-dimethyl-7,13-diaza-1,4,10-trioxacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / K₂CO₃, tetrabutylammonium chloride / dimethylformamide / 12 h / 80 °C

2: 1.) Na, NH₃

With tetrabutyl-ammonium chloride; ammonia; sodium; potassium carbonate; In N,N-dimethyl-formamide;