C₄₄H₅₆O₁₂

Base Information

Chemical Name:C₄₄H₅₆O₁₂
CAS No.:1400765-86-7
Molecular Formula:C₄₄H₅₆O₁₂
Molecular Weight:776.921
Hs Code.:

C<sub>44</sub>H<sub>56</sub>O<sub>12</sub>

Synonyms:C₄₄H₅₆O₁₂

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Chemical Property of C₄₄H₅₆O₁₂

Chemical Property:

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Technology Process of C₄₄H₅₆O₁₂

There total 5 articles about C₄₄H₅₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1258540-93-0
C₁₉H₂₅IO₄

: 1400765-79-8
C₂₅H₃₂O₈

: 1400765-86-7
C₄₄H₅₆O₁₂

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 20 ℃; for 20h; Darkness; Inert atmosphere;
DOI:10.1021/ja306596m

Reference yield:

: 32437-88-0
6-<(tetrahydropyranyl)oxy>hexanoic acid

: 1400765-86-7
C₄₄H₅₆O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1: diisopropyl-carbodiimide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C / Darkness; Inert atmosphere

2: toluene-4-sulfonic acid / methanol; dichloromethane / 2.5 h / 20 °C

3: diisopropyl-carbodiimide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C / Darkness; Inert atmosphere

4: toluene-4-sulfonic acid / methanol; dichloromethane / 3.5 h / 20 °C

5: pyridine; dmap / dichloromethane / 24 h / 20 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triethylamine / tetrahydrofuran / 20 h / 20 °C / Darkness; Inert atmosphere

With pyridine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; 6: |Sonogashira Cross-Coupling;
DOI:10.1021/ja306596m

Reference yield:

: 1400765-75-4
C₁₅H₁₈O₃

: 1400765-86-7
C₄₄H₅₆O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1: diisopropyl-carbodiimide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C / Darkness; Inert atmosphere

2: toluene-4-sulfonic acid / methanol; dichloromethane / 3.5 h / 20 °C

3: pyridine; dmap / dichloromethane / 24 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triethylamine / tetrahydrofuran / 20 h / 20 °C / Darkness; Inert atmosphere

With pyridine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; 4: |Sonogashira Cross-Coupling;
DOI:10.1021/ja306596m