2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide

Base Information

Chemical Name:2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide
CAS No.:99121-63-8
Molecular Formula:C₂₂H₂₂N₄O₄
Molecular Weight:406.441
Hs Code.:

Synonyms:2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide

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Chemical Property of 2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide

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Technology Process of 2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide

There total 5 articles about 2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.5%

: 87497-77-6,99121-61-6
2,5-dibenzyl-3a,6a-diethoxycarbonyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole

: 87497-81-2,99121-63-8
2,5-dibenzyl-3a,6a-dicarbamoyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole

Guidance literature:: With ammonia; In ethanol; at 100 ℃; for 72h;

Reference yield: 25.4%

: diethyl 2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxylate

: 99121-62-7
2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a-carboxamide

: 99121-63-8
2,5-dibenzyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole-3a,6a-dicarboxamide

Guidance literature:: With ammonia; In ethanol; at 100 ℃; for 75h;
DOI:10.1002/hlca.19850680312

Reference yield:

: 632-56-4
tetraethyl ethane-1,1,2,2-tetracarboxylate

: 87497-81-2,99121-63-8
2,5-dibenzyl-3a,6a-dicarbamoyl-1,4-dioxo-octahydropyrrolo<3,4-c>pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 83.5 percent / trifluoroacetic acid / 100 °C

2: 58.5 percent / ammonia / ethanol / 72 h / 100 °C

With ammonia; trifluoroacetic acid; In ethanol;