5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

Base Information

Chemical Name:5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-
CAS No.:1262615-41-7
Molecular Formula:C₆₅H₅₀F₂O₁₄
Molecular Weight:1093.1
Hs Code.:

Synonyms:5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

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Technology Process of 5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

There total 8 articles about 5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 456-22-4
4-Fluorobenzoic acid

: 1262615-38-2
5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-(3'',4''-O-isopropylidene)galactosyl-4H-chromen-4-one

: 1262615-41-7
5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm200010x

Reference yield: 71.0%

: 1262615-41-7
5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

Guidance literature:

Reference yield:

: 1262615-36-0
5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-tetraacetylgalactosyl-4H-chromen-4-one

: 1262615-41-7
5,7-dibenzyloxy-2-(2,2-diphenylbenzo[d][1,3]dioxol-5-yl)-3-β-D-[2'',6''-di-O-(4-fluorobenzoyl)-3'',4''-O-isopropylidene]galactosyl-4H-chromen-

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / ethyl acetate / 1.5 h / 20 °C

1.2: H⁺ion exchange resin

2.1: sulfuric acid; copper(II) sulfate / 12 h / 20 °C

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / -10 - 20 °C / Inert atmosphere

With dmap; sulfuric acid; sodium methylate; copper(II) sulfate; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate;
DOI:10.1021/jm200010x