4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

Base Information

Chemical Name:4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate
CAS No.:1342883-85-5
Molecular Formula:C₃₈H₃₈N₂O₅
Molecular Weight:602.73
Hs Code.:

Synonyms:4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

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Chemical Property of 4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

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Technology Process of 4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

There total 4 articles about 4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 20651-71-2
4-butyl benzoic acid

: 1342883-62-8
4-[3-(4-hydroxyphenyl)-1,2,4-oxadiazol-5-yl]phenyl 4-hexyl-benzoate

: 1342883-85-5
4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.039

Reference yield:

: 62536-94-1
4-benzyloxy-N'-hydroxybenzimidamide

: 1342883-85-5
4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide / 1,4-dioxane / 9 h / 25 °C / Reflux

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethyl acetate / 6 h / 20 °C / 750.08 Torr

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C / Inert atmosphere

With dmap; palladium 10% on activated carbon; hydrogen; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; ethyl acetate;
DOI:10.1016/j.tet.2011.09.039

Reference yield:

: 52805-36-4
4-benzyloxybenzonitrile

: 1342883-85-5
4-{3-[4-(4-n-butylbenzoyloxy)phenyl]-1,2,4-oxadiazol-5-yl}phenyl 4-hexylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride

2: dicyclohexyl-carbodiimide / 1,4-dioxane / 9 h / 25 °C / Reflux

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethyl acetate / 6 h / 20 °C / 750.08 Torr

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C / Inert atmosphere

With dmap; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; ethyl acetate;
DOI:10.1016/j.tet.2011.09.039