(1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin

Base Information

Chemical Name:(1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin
CAS No.:105787-03-9
Molecular Formula:C₂₄H₂₆N₂
Molecular Weight:342.484
Hs Code.:

Synonyms:(1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin

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Chemical Property of (1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin

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Technology Process of (1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin

There total 2 articles about (1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 498-66-8
norbornene

: 30169-45-0
4,4-dimethyl-3,5-diphenyl-4H-pyrazole

: 105787-03-9
(1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin

Guidance literature:: With trifluoroacetic acid; In chloroform; for 72h; Heating;

Reference yield:

: 41169-42-0
2,2-dimethyl-1,3-diphenylpropane-1,3-dione

: 105787-03-9
(1α,4α,4aα,5β,8β,8aα)-1,4,4a,5,6,7,8,8a-Octahydro-1,4-diphenyl-9,9-dimethyl-1,4:5,8-dimethanophthalazin

Guidance literature:: Multi-step reaction with 2 steps

1: H₂NNH₂*H₂O / CH₂Cl₂ / 3 h / Heating

2: 12 percent / CF₃-COOH / CHCl₃ / 72 h / Heating

With hydrazine hydrate; trifluoroacetic acid; In dichloromethane; chloroform;