5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

Base Information

Chemical Name:5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene
CAS No.:272445-59-7
Molecular Formula:C₅₆H₅₀N₂O₄
Molecular Weight:815.024
Hs Code.:

Synonyms:5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

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Chemical Property of 5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

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Technology Process of 5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

There total 3 articles about 5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 272445-56-4
N,N'-dibutyl-1,6,7,12-tetraphenoxyperylene-3,4:9,10-tetracarboxylic acid bisimide

: 272445-59-7
5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; for 3h; Heating;
DOI:10.1002/(SICI)1521-3773(20000403)39:7<1243::AID-ANIE1243>3.0.CO;2-Z

Reference yield:

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: 272445-59-7
5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / propionic acid / 8 h / 140 °C

2: 53 percent / potassium carbonate; 1-methyl-2-pyrrolidinone / 16 h / 130 °C

3: 50 percent / lithium aluminum hydride; aluminum chloride / tetrahydrofuran / 6 h / 35 °C

With 1-methyl-pyrrolidin-2-one; lithium aluminium tetrahydride; aluminium trichloride; potassium carbonate; propionic acid; In tetrahydrofuran;
DOI:10.1021/jo011133l

Reference yield:

: 95689-64-8
N,N’-dibutyl-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid bisimide

: 272445-59-7
5,6,12,13-tetraphenoxy-1,3,8,10-tetrahydro-2,9-dibutyl-2,9-diazadibenzo[cd,lm]perylene

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / potassium carbonate; 1-methyl-2-pyrrolidinone / 16 h / 130 °C

2: 50 percent / lithium aluminum hydride; aluminum chloride / tetrahydrofuran / 6 h / 35 °C

With 1-methyl-pyrrolidin-2-one; lithium aluminium tetrahydride; aluminium trichloride; potassium carbonate; In tetrahydrofuran;
DOI:10.1021/jo011133l