N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide

Base Information

• Chemical Name: N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide
• CAS No.: 1221178-52-4
• Molecular Formula: C₃₁H₄₄N₂O₄SSi
• Molecular Weight: 568.853

Synonyms:N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide

Chemical Property of N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide

Chemical Property:

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Technology Process of N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide

There total 2 articles about N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-benzyl-N-(3-((1R)-2-iodo-1-triethylsilyloxy-ethyl)phenyl)methanesulfonamide (320728-11-8) + N-Benzylethanolamine (104-63-2) → N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide (1221178-52-4)

Guidance literature:

In neat (no solvent); at 100 ℃; Inert atmosphere;

DOI:10.1021/acs.jmedchem.5b00638

Reference yield:

N-Benzylethanolamine (104-63-2) → N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide (1221178-52-4)

Guidance literature:

Reference yield:

N-benzyl-N-(3-((1R)-2-(benzyl(2-hydroxyethyl)amino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide (1221178-52-4) → N-(3-((1R)-2-(2-hydroxyethylamino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide (1221179-00-5)

Guidance literature:

With hydrogen; 20 % Pd(OH)2/C; In tetrahydrofuran; methanol; at 50 ℃; for 15h; Inert atmosphere;

upstream raw materials:

N-Benzylethanolamine

N-benzyl-N-(3-((1R)-2-iodo-1-triethylsilyloxy-ethyl)phenyl)methanesulfonamide

Downstream raw materials:

(R)-[3-[2-[N-benzyl-N-[2-(2-ethoxycarbonyl-3-methyl-1H-indol-6-yloxy)ethyl]amino]-1-triethylsilyloxyethyl]phenyl](methylsulfonyl)benzylamine

N-(3-((1R)-2-(2-hydroxyethylamino)-1-triethylsilyloxyethyl)phenyl)methanesulfonamide

(R)-tert-butyl 6-(2-(tert-butoxycarbonyl(2-(3-(N-(tert-butoxycarbonyl)(methyl)sulfonamido)phenyl)-2-(triethylsilyloxy)ethyl)amino)ethoxy)-3-ethylindazole-1-carboxylate

(R)-tert-butyl 6-(2-(tert-butoxycarbonyl-(2-(3-(N-(tert-butoxycarbonyl)(methyl)sulfonamido)phenyl)-2-(triethylsilyloxy)ethyl)amino)ethoxy)-3-isopropylindazole-1-carboxylate

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