2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

Base Information

Chemical Name:2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene
CAS No.:1370619-02-5
Molecular Formula:C₃₈H₄₂O₁₁
Molecular Weight:674.745
Hs Code.:

Synonyms:2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

Chemical Property:

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Technology Process of 2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

There total 8 articles about 2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370619-06-9
2-(4'-butoxyphenyl)-5-bromotoluene

: 1370619-02-5
2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 3 h / Reflux

2: acetone / 4 h / Reflux

3: sodium hydroxide / water / 24 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; hydroquinone / ethanol; water; benzene / 6 h / Inert atmosphere; Reflux

5: hydrogenchloride; water / tetrahydrofuran; methanol / 4 h / 20 °C

6: quinoline; calcium sulfate; silver(l) oxide / ethyl acetate / 48 h / 20 °C / Darkness

With quinoline; hydrogenchloride; calcium sulfate; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium carbonate; hydroquinone; sodium hydroxide; silver(l) oxide; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; water; ethyl acetate; acetone; benzene;
DOI:10.1039/c2cc00036a

Reference yield:

: C₁₇H₁₈Br₂O

: 1370619-02-5
2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

Guidance literature:: Multi-step reaction with 5 steps

1: acetone / 4 h / Reflux

2: sodium hydroxide / water / 24 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; hydroquinone / ethanol; water; benzene / 6 h / Inert atmosphere; Reflux

4: hydrogenchloride; water / tetrahydrofuran; methanol / 4 h / 20 °C

5: quinoline; calcium sulfate; silver(l) oxide / ethyl acetate / 48 h / 20 °C / Darkness

With quinoline; hydrogenchloride; calcium sulfate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium carbonate; hydroquinone; sodium hydroxide; silver(l) oxide; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; acetone; benzene;
DOI:10.1039/c2cc00036a

Reference yield:

: 1370619-07-0
2-(4'-butoxyphenyl)-5-bromostyrene

: 1370619-02-5
2-(4'-butoxyphenyl)-5-[4'-(2,3,4,6-tetra-O-acetyl-β-D-galactosyloxy)phenyl]styrene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; hydroquinone / ethanol; water; benzene / 6 h / Inert atmosphere; Reflux

2: hydrogenchloride; water / tetrahydrofuran; methanol / 4 h / 20 °C

3: quinoline; calcium sulfate; silver(l) oxide / ethyl acetate / 48 h / 20 °C / Darkness

With quinoline; hydrogenchloride; calcium sulfate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium carbonate; hydroquinone; silver(l) oxide; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; benzene;
DOI:10.1039/c2cc00036a