N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

Base Information

Chemical Name:N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide
CAS No.:380652-86-8
Molecular Formula:C₂₂H₁₆N₂O₄S
Molecular Weight:404.446
Hs Code.:

Synonyms:N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

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Chemical Property of N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

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Technology Process of N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

There total 4 articles about N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 850189-76-3
N-(3'-chloro-1',4'-dioxo-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

: 62-53-3
aniline

: 380652-86-8
N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

Guidance literature:: N-(3'-chloro-1',4'-dioxo-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide; With cerium(III) chloride; In toluene; for 1h;

aniline; In toluene; at 110 ℃; for 48h;
DOI:10.1021/ja909165u

Reference yield:

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 380652-86-8
N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / toluene

2.1: cerium(III) chloride heptahydrate / toluene / 1 h

2.2: 48 h / 110 °C

With cerium(III) chloride heptahydrate; caesium carbonate; In toluene;

Reference yield:

: 98-10-2
benzenesulfonamide

: 380652-86-8
N-(1',4'-dioxo-3'-(phenylamino)-1',4'-dihydronaphthalen-2'-yl)benzenesulphonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / toluene

2.1: cerium(III) chloride heptahydrate / toluene / 1 h

2.2: 48 h / 110 °C

With cerium(III) chloride heptahydrate; caesium carbonate; In toluene;