Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate

Base Information

• Chemical Name: Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate
• CAS No.: 71725-03-6
• Molecular Formula: C₂₅H₃₁NO₅
• Molecular Weight: 425.525

Synonyms:Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate

Chemical Property of Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate

Chemical Property:

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Technology Process of Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate

There total 3 articles about Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2,4-dibromobutyric acid tert-butyl ester (77629-96-0,71725-02-5) + Ethyl α-Amino-p-(benzyloxy)-phenylacetate (70875-50-2) → Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate (71725-03-6)

Guidance literature:

With sodium carbonate; In ethanol; at 55 ℃; for 96h;

DOI:10.1021/jo00328a001

Reference yield:

2-glycine Ethyl Ester Hydrotosylate (70875-51-3) + 2,4-dibromobutyric acid tert-butyl ester (77629-96-0,71725-02-5) → Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate (71725-03-6)

Guidance literature:

With sodium carbonate; In acetonitrile; at 50 ℃; for 96h; Yield given;

DOI:10.1021/jo00328a002

Reference yield:

→ Ethyl α--2-(carbo-tert-butoxy)-1-azetidineacetate (71725-03-6)

Guidance literature:

Butyrat I, α-Aminoester IIb;

upstream raw materials:

2-glycine Ethyl Ester Hydrotosylate

2,4-dibromobutyric acid tert-butyl ester

Ethyl α-Amino-p-(benzyloxy)-phenylacetate

Downstream raw materials:

Ethyl α--2-oxo-1-azetidineacetate

Diethyl 3-Azido-α--2-oxo-1-azetidinemalonate

Diethyl α--2-oxo-1-azetidinemalonate

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