C₂₇H₃₆⁽²⁾H₂N₆O₉

Base Information

Chemical Name:C₂₇H₃₆⁽²⁾H₂N₆O₉
CAS No.:874305-93-8
Molecular Formula:C₂₇H₃₈N₆O₉
Molecular Weight:592.618
Hs Code.:

C<sub>27</sub>H<sub>36</sub><sup>(2)</sup>H<sub>2</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₂₇H₃₆⁽²⁾H₂N₆O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₆⁽²⁾H₂N₆O₉

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Technology Process of C₂₇H₃₆⁽²⁾H₂N₆O₉

There total 8 articles about C₂₇H₃₆⁽²⁾H₂N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: GPGGG-OCH₂Ph hydrochloride

: 42492-65-9
N-(tert-butoxycarbonyl)glycine-2,2-d₂

: 874305-93-8
C₂₇H₃₆⁽²⁾H₂N₆O₉

Guidance literature:: With 4-methyl-morpholine; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1021/ja0558894

Reference yield:

: 874305-85-8
Boc-GPGGG-OCH₂Ph

: 874305-93-8
C₂₇H₃₆⁽²⁾H₂N₆O₉

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / dioxane / 0.5 h / 5 °C

2: 82 percent / 1-hydroxybenzotriazole hydrate; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; NMM / CH₂Cl₂ / 20 °C

With 4-methyl-morpholine; hydrogenchloride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ja0558894

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 874305-93-8
C₂₇H₃₆⁽²⁾H₂N₆O₉

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / Et₃N; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 72 h / 20 °C

2: 100 percent / HCl / dioxane / 1 h / 5 °C

3: 90 percent / 1-hydroxybenzotriazole hydrate; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; NMM / CH₂Cl₂ / 20 °C

4: HCl / dioxane / 0.5 h / 5 °C

5: 82 percent / 1-hydroxybenzotriazole hydrate; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; NMM / CH₂Cl₂ / 20 °C

With 4-methyl-morpholine; hydrogenchloride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ja0558894