Technology Process of NEt-3IP
There total 8 articles about NEt-3IP which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C21H28N2O3;
With
water; sodium hydroxide;
In
methanol;
at 60 ℃;
for 0.666667h;
With
water; ammonium chloride;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
2.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
3.1: acetic acid / 8 h / 80 °C
3.2: 18 h / 90 °C / Reflux
4.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h
4.2: 2 h
5.1: water; sodium hydroxide / methanol / 0.67 h / 60 °C
With
hydrogenchloride; water; hydrogen; sodium hydride; potassium carbonate; acetic acid; potassium iodide; sodium hydroxide;
palladium on activated charcoal;
In
methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid; water; sodium nitrite / 0 - 5 °C
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
3.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
4.1: acetic acid / 8 h / 80 °C
4.2: 18 h / 90 °C / Reflux
5.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h
5.2: 2 h
6.1: water; sodium hydroxide / methanol / 0.67 h / 60 °C
With
hydrogenchloride; sulfuric acid; water; hydrogen; sodium hydride; potassium carbonate; acetic acid; potassium iodide; sodium hydroxide; sodium nitrite;
palladium on activated charcoal;
In
methanol; water; N,N-dimethyl-formamide;
