tert-butyl N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate

Base Information

• Chemical Name: tert-butyl N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate
• CAS No.: 1182206-80-9
• Molecular Formula: C₃₉H₄₁N₇O₈
• Molecular Weight: 735.797

Synonyms:tert-butyl N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate

Chemical Property of tert-butyl N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate

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Technology Process of tert-butyl N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate

There total 1 articles about tert-butyl N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

ethyl 2-(2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazine)acetate (1182206-85-4) + tert-butyl N6-[(benzyloxy)carbonyl]-8-(bromomethyl)adenine-9-acetate (1182206-91-2) → tert-butyl N6-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate (1182206-80-9)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1002/hlca.200900047

Reference yield: 98.0%

tert-butyl N6-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate (1182206-80-9) → N6-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetic acide (1182206-93-4)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1002/hlca.200900047

Reference yield: 87.0%

tert-butyl N6-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetate (1182206-80-9) → tert-butyl N6-[(benzyloxy)carbonyl]-8-{[1-(2-ethoxy-2-oxoethyl)hydrazino]methyl}adenine-9-acetate (1182206-92-3)

Guidance literature:

With piperidine; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

DOI:10.1002/hlca.200900047

upstream raw materials:

ethyl 2-(2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazine)acetate

tert-butyl N₆-[(benzyloxy)carbonyl]-8-(bromomethyl)adenine-9-acetate

Downstream raw materials:

tert-butyl N₆-[(benzyloxy)carbonyl]-8-{[1-(2-ethoxy-2-oxoethyl)hydrazino]methyl}adenine-9-acetate

N₆-[(benzyloxy)carbonyl]-8-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]adenine-9-acetic acide

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