Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

Base Information

Chemical Name:Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat
CAS No.:142842-68-0
Molecular Formula:C₂₁H₁₃N₃O₄S₃
Molecular Weight:467.55
Hs Code.:

Synonyms:Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

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Chemical Property of Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

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Technology Process of Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

There total 5 articles about Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 142842-67-9
Methyl-7-chloroformyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-7-carboxylat

: 142842-68-0
Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

Guidance literature:: With sodium azide; In water; acetone; for 1h; Ambient temperature;

Reference yield:

: 139101-75-0
Methyl-5-hydroxy-2,2-diphenyl-4H-1,3-dithiin-6-carboxylat

: 142842-68-0
Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / HCl, H₂S / ethanol; tetrahydrofuran / 12 h

2: piperidine acetate / benzene / 1 h / Heating

3: 91 percent / p-toluenesulfonic acid monohydrate / toluene / 0.17 h / Heating

4: 90 percent / thionyl chloride / 0.08 h / Heating

5: 87 percent / NaN₃ / acetone; H₂O / 1 h / Ambient temperature

With hydrogenchloride; thionyl chloride; sodium azide; hydrogen sulfide; piperdinium acetate; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; water; acetone; toluene; benzene;

Reference yield:

: 142842-61-3
Methyl-5-mercapto-2,2-diphenyl-4H-1,3-dithiin-6-carboxylat

: 142842-68-0
Methyl-7-azidocarbonyl-6-oxo-2,2-diphenyl-6H-thieno<3,2-d>-1,3-dithiin-4-carboxylat

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine acetate / benzene / 1 h / Heating

2: 91 percent / p-toluenesulfonic acid monohydrate / toluene / 0.17 h / Heating

3: 90 percent / thionyl chloride / 0.08 h / Heating

4: 87 percent / NaN₃ / acetone; H₂O / 1 h / Ambient temperature

With thionyl chloride; sodium azide; piperdinium acetate; toluene-4-sulfonic acid; In water; acetone; toluene; benzene;