{(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu

Base Information

Chemical Name:{(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu
CAS No.:112088-20-7
Molecular Formula:C₄₁H₂₈ClF₉N₄PRu*ClO₄
Molecular Weight:1014.63
Hs Code.:

{(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2{P(C<sub>6</sub>H<sub>4</sub>CF<sub>3</sub>)3}RuCl}<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=C<sub>41</sub>H<sub>28</sub>Cl<sub>2</sub>F<sub>9</sub>O<sub>4</sub>N<sub>4</sub>PRu

Synonyms:{(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu

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Chemical Property of {(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu

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Technology Process of {(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu

There total 1 articles about {(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

: sodium perchlorate

: 13406-29-6
tris(para-trifluoromethyl)phenyl phosphine

: 112088-20-7
{(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu

Guidance literature:: In ethanol; water; cis-Ru(bpy)2Cl2.2H2O and P(C6H4CF3-p)3 in aq.EtOH refluxed 8 h, evapd. to dryness, H2O added, pptd. by excess NaClO4; filtered, purifn. by Al2O3/1:1 toluene/acetonitrile chromy., dissoln. in acetone and repptn. with ether;
DOI:10.1021/ja00213a019

Reference yield:

: 112088-20-7
{(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₄₁H₂₈Cl₂F₉O₄N₄PRu

: 7732-18-5
water

: silver perchlorate

: 112088-36-5
{(C₁₀H₈N₂)2{P(C₆H₄CF₃)3}Ru(OH₂)}⁽²⁺⁾*2ClO₄^(1-)=C₄₁H₃₀Cl₂O₉N₄PRuF₉

Guidance literature:: In water; byproducts: AgCl; refluxing the chloro analogue of the complex with AgClO4 in H2O for 1.5 h with AgCl pptn., AgCl filtered off; pptn. by 70% HClO4, filtration, washed with cold water;
DOI:10.1021/ja00213a019