C₅₂H₄₄N₂

Base Information

Chemical Name:C₅₂H₄₄N₂
CAS No.:1453122-32-1
Molecular Formula:C₅₂H₄₄N₂
Molecular Weight:696.935
Hs Code.:

C<sub>52</sub>H<sub>44</sub>N<sub>2</sub>

Synonyms:C₅₂H₄₄N₂

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Chemical Property of C₅₂H₄₄N₂

Chemical Property:

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Technology Process of C₅₂H₄₄N₂

There total 6 articles about C₅₂H₄₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 25069-74-3
N,N-diphenyl-N-(4-vinylphenyl)amine

: 1548389-23-6
C₃₃H₂₈F₃NO₃S

: 1453122-32-1
C₅₂H₄₄N₂

Guidance literature:: With palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl acetamide; at 85 ℃; for 4h;

Reference yield:

: 89057-44-3
5,5,10,10-Tetramethyl-5,10-dihydroindeno<2,1-a>inden

: 1453122-32-1
C₅₂H₄₄N₂

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h / 20 °C

2: aluminum (III) chloride / dichloromethane / 24 h / 0 - 20 °C

3: 3-chloro-benzenecarboperoxoic acid / chloroform / 72 h / 0 - 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butylphosphine; potassium tert-butylate / toluene / 4 h / 85 °C

5: potassium phosphate / toluene / 0.5 h / 0 - 20 °C

6: palladium diacetate; tris-(o-tolyl)phosphine; triethylamine / N,N-dimethyl acetamide / 4 h / 85 °C

With aluminum (III) chloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; tri-tert-butylphosphine; potassium tert-butylate; palladium diacetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; tris-(o-tolyl)phosphine; In dichloromethane; chloroform; N,N-dimethyl acetamide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1548389-02-1
C₂₂H₂₁BrO

: 1453122-32-1
C₅₂H₄₄N₂

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 72 h / 0 - 20 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butylphosphine; potassium tert-butylate / toluene / 4 h / 85 °C

3: potassium phosphate / toluene / 0.5 h / 0 - 20 °C

4: palladium diacetate; tris-(o-tolyl)phosphine; triethylamine / N,N-dimethyl acetamide / 4 h / 85 °C

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butylphosphine; potassium tert-butylate; palladium diacetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; tris-(o-tolyl)phosphine; In chloroform; N,N-dimethyl acetamide; toluene;