C₂₆H₃₇NO₈

Base Information

Chemical Name:C₂₆H₃₇NO₈
CAS No.:1276043-19-6
Molecular Formula:C₂₆H₃₇NO₈
Molecular Weight:491.582
Hs Code.:

C<sub>26</sub>H<sub>37</sub>NO<sub>8</sub>

Synonyms:C₂₆H₃₇NO₈

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Chemical Property of C₂₆H₃₇NO₈

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Technology Process of C₂₆H₃₇NO₈

There total 10 articles about C₂₆H₃₇NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: C₃₂H₅₁NO₈Si

: C₂₂H₂₆O₈

: 1276043-19-6
C₂₆H₃₇NO₈

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; Inert atmosphere;
DOI:10.1007/s11426-010-4176-8

Reference yield:

: 2-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-benzoic acid

: C₂₂H₂₆O₈

: 1276043-19-6
C₂₆H₃₇NO₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 °C / Inert atmosphere; Cooling with ice

2.1: dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran; cyclohexane / 0.75 h / -78 °C / Inert atmosphere

3.2: 3.5 h / -78 - 20 °C / Inert atmosphere

4.1: potassium hydroxide / tetrahydrofuran; methanol; water / 20 °C / Inert atmosphere

With oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water;
DOI:10.1007/s11426-010-4176-8

Reference yield:

: 960078-67-5
C₃₀H₄₀O₅Si

: C₂₂H₂₆O₈

: 1276043-19-6
C₂₆H₃₇NO₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 22 h / 20 °C / Inert atmosphere

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 21 h / 20 °C / Inert atmosphere

3.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran; cyclohexane / 0.75 h / -78 °C / Inert atmosphere

3.2: 3.5 h / -78 - 20 °C / Inert atmosphere

4.1: potassium hydroxide / tetrahydrofuran; methanol; water / 20 °C / Inert atmosphere

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; sec.-butyllithium; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water;
DOI:10.1007/s11426-010-4176-8