benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

Base Information

Chemical Name:benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine
CAS No.:869101-62-2
Molecular Formula:C₄₂H₄₇NO₄
Molecular Weight:629.839
Hs Code.:

Synonyms:benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

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Chemical Property of benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

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Technology Process of benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

There total 8 articles about benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzyl-[5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pent-(E)-ylidene]-amine

: 869101-62-2
benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

Guidance literature:: With sodium cyanoborohydride; In methanol; dichloromethane; at 20 ℃; for 89h;
DOI:10.1016/j.bmc.2005.06.058

Reference yield:

: O,O-di-t-butyloxycarbonylcurcumin

: 869101-62-2
benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 92.1 percent / H₂ / Pd/C / ethyl acetate / 60 h / 20 °C / 10343 Torr

2.1: trifluoroacetic acid / CH₂Cl₂ / 20 h / 14 °C

2.2: 51.5 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760 Torr

3.1: 99 percent / potassium carbonate / dimethylformamide / 0.25 h / microwave irradiation

4.1: HCl / methanol; CH₂Cl₂ / 0.5 h / 20 °C

5.1: 211 mg / NaBH₃CN / methanol; CH₂Cl₂ / 89 h / 20 °C

With hydrogenchloride; hydrogen; sodium cyanoborohydride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.06.058

Reference yield:

: 458-37-7
curcumin

: 869101-62-2
benzyl-{5-(4-benzyloxy-3-methoxy-phenyl)-1-[2-(4-benzyloxy-3-methoxy-phenyl)-ethyl]-pentyl}-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: 88.7 percent / NaOH / methanol / 3 h / 20 °C

2.1: 92.1 percent / H₂ / Pd/C / ethyl acetate / 60 h / 20 °C / 10343 Torr

3.1: trifluoroacetic acid / CH₂Cl₂ / 20 h / 14 °C

3.2: 51.5 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760 Torr

4.1: 99 percent / potassium carbonate / dimethylformamide / 0.25 h / microwave irradiation

5.1: HCl / methanol; CH₂Cl₂ / 0.5 h / 20 °C

6.1: 211 mg / NaBH₃CN / methanol; CH₂Cl₂ / 89 h / 20 °C

With hydrogenchloride; sodium hydroxide; hydrogen; sodium cyanoborohydride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.06.058