allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside
CAS No.:652149-18-3
Molecular Formula:C₄₇H₄₉NO₁₈
Molecular Weight:915.902
Hs Code.:

Synonyms:allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

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Technology Process of allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

There total 1 articles about allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 215102-68-4
allyl 2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

: 652149-18-3
allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1.5h;
DOI:10.1016/S0008-6215(03)00292-1

Reference yield:

: 545-06-2
trichloroacetonitrile

: 652149-18-3
allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

: (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranosyl trichloroacetimidate

: (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside; With sodium acetate; palladium dichloride; In acetic acid; Irradiation;

trichloroacetonitrile; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1.5h; Title compound not separated from byproducts;
DOI:10.1016/S0008-6215(03)00292-1

Reference yield:

: 652149-18-3
allyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranoside

: (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-β-D-glucopyranose

: (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-deoxy-3,4-di-O-p-methylbenzoyl-2-phthalimido-α-D-glucopyranose

Guidance literature:: With sodium acetate; palladium dichloride; In acetic acid; Title compound not separated from byproducts; Irradiation;
DOI:10.1016/S0008-6215(03)00292-1