[(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]

Base Information

Chemical Name:[(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]
CAS No.:1337898-05-1
Molecular Formula:C₄₈H₂₈F₁₀N₂P₂PdPt
Molecular Weight:1186.2
Hs Code.:

Synonyms:[(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]

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Chemical Property of [(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]

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Technology Process of [(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]

There total 1 articles about [(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 14783-10-9
[palladium(II)dichloride(1,10-phenanthroline)]

: cis-bis(diphenylphosphine)bis(pentafluorophenyl)platinum(II)

: 1337898-05-1
[(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]

Guidance literature:: With butyllithium; In tetrahydrofuran; hexane; C4H9Li in hexane was added under Ar to a soln. of Pt-complex in THF at ca. -78°C, stirred for 15 min, Pd-complex was added, room temp. for 16 h; evapd. to dryness, CH2Cl2 was added, filtered, evapd., methanol was added, crystals were filtered off, washed with methanol; elem. anal.;
DOI:10.1021/ic201354s

Reference yield: 89.0%

: 73165-02-3,623171-38-0
perchlorato(triphenylphosphane)silver(I)

: 1337898-05-1
[(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)]

: [(C6F5)2Pt(μ-PPh2)2Pd(1,10-phenanthroline)Ag(PPh3)]ClO4

Guidance literature:: In dichloromethane; Ag(OClO3)(P(C6H5)3) was added to a soln. of complex in CH2Cl2, stirred at room temp. for 30 min with the exclusion of light; evapd., hexane was added, crystals were filtered, washed with hexane (twice); elem. anal.;
DOI:10.1021/ic201354s