methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate

Base Information

Chemical Name:methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate
CAS No.:1116228-35-3
Molecular Formula:C₁₃H₁₅ClFNO₄
Molecular Weight:303.718
Hs Code.:

Synonyms:methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate

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Chemical Property of methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate

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Technology Process of methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate

There total 1 articles about methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 940054-42-2
(3-chloro-5-fluorophenyl)-carbamic acid tert-butyl ester

: 79-22-1
methyl chloroformate

: 1116228-35-3
methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate

: 1116228-38-6
1,1-dimethylethyl [5-chloro-2-(2,2-dimethylpropanoyl)-3-fluorophenyl]carbamate

Guidance literature:: (3-chloro-5-fluorophenyl)-carbamic acid tert-butyl ester; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 3h;

methyl chloroformate; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

With water; ammonium chloride; In tetrahydrofuran; pentane; at -78 ℃;

Reference yield: 69.0%

: 1116228-35-3
methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate

: 940054-48-8
2-amino-4-chloro-6-fluorobenzoic acid

Guidance literature:: methyl 4-chloro-2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-6-fluorobenzoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 72h;

With hydrogenchloride; In water; at 20 ℃; pH=2;