C₆₃H₈₄O₁₂Si₂

Base Information

Chemical Name:C₆₃H₈₄O₁₂Si₂
CAS No.:1265446-50-1
Molecular Formula:C₆₃H₈₄O₁₂Si₂
Molecular Weight:1089.52
Hs Code.:

C<sub>63</sub>H<sub>84</sub>O<sub>12</sub>Si<sub>2</sub>

Synonyms:C₆₃H₈₄O₁₂Si₂

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Chemical Property of C₆₃H₈₄O₁₂Si₂

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Technology Process of C₆₃H₈₄O₁₂Si₂

There total 13 articles about C₆₃H₈₄O₁₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₁H₈₂O₁₁Si₂

: 108-24-7
acetic anhydride

: 1265446-50-1
C₆₃H₈₄O₁₂Si₂

Guidance literature:: With pyridine; dmap; In hexane; dichloromethane; at -78 - 0 ℃;
DOI:10.1021/np100729d

Reference yield:

: 1265446-25-0
C₁₆H₂₂O₆

: 1265446-50-1
C₆₃H₈₄O₁₂Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / tetrahydrofuran / 0 - 20 °C

2: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 1 h / 20 °C

3: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C

4: pyridine; dmap / hexane; dichloromethane / -78 - 0 °C

With pyridine; 1H-imidazole; dmap; 2,4,6-trichlorobenzoyl chloride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/np100729d

Reference yield:

: 602301-65-5
(2R,4aR,6S,7R,8aS)-2-(4-Methoxy-phenyl)-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1265446-50-1
C₆₃H₈₄O₁₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: 1H-imidazole / tetrahydrofuran / 0 - 20 °C

3.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 1 h / 20 °C

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C

5.1: pyridine; dmap / hexane; dichloromethane / -78 - 0 °C

With pyridine; 1H-imidazole; dmap; 2,4,6-trichlorobenzoyl chloride; bis-(1,2-dimethylpropyl)borane; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/np100729d