(2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

Base Information

Chemical Name:(2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol
CAS No.:596096-87-6
Molecular Formula:C₂₆H₂₆O₂S₂
Molecular Weight:434.623
Hs Code.:

Synonyms:(2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

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Chemical Property of (2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

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Technology Process of (2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

There total 1 articles about (2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32364-72-0
[2,2']bithiophenyl-5,5'-dicarbaldehyde

: 576-22-7
2-Bromo-m-xylene

: 596096-87-6
(2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

Guidance literature:: 2-Bromo-m-xylene; With magnesium; In tetrahydrofuran;

[2,2']bithiophenyl-5,5'-dicarbaldehyde; In tetrahydrofuran; at 0 ℃; for 4h; Further stages.;
DOI:10.1002/chem.200204537

Reference yield: 65.0%

: 109-97-7,30604-81-0
pyrrole

: 596096-87-6
(2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

: 596096-89-8
C₃₄H₃₂N₂S₂

Guidance literature:: With trifluoroacetic acid;
DOI:10.1002/chem.200204537

Reference yield:

: 596096-87-6
(2,6-dimethyl-phenyl)-{5'-[(2,6-dimethyl-phenyl)-hydroxy-methyl]-[2,2']bithiophenyl-5-yl}-methanol

: C₆₈H₅₄N₄S₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: 65 percent / TFA

2.1: TFA / CH₂Cl₂

2.2: 5 percent / chloranil / CH₂Cl₂ / Heating

With trifluoroacetic acid; In dichloromethane;
DOI:10.1002/chem.200204537