N-DECYL-D21 ALCOHOL

Base Information

• Chemical Name: N-DECYL-D21 ALCOHOL
• CAS No.: 110510-78-6
• Molecular Formula: C₁₀H₂₂O
• Molecular Weight: 179.117
• Mol file: 110510-78-6.mol

Synonyms:N-DECANOL (D21);N-DECYL-D21 ALCOHOL

Chemical Property of N-DECYL-D21 ALCOHOL

Chemical Property:

• Melting Point: 179.4 °C
• PSA: 20.23000
• LogP: 3.11940

Purity/Quality:

98% ^*data from raw suppliers

1-Decanol-d21 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1-Decanol-d21, is the labeled analogue of 1-Decanol (D212540), which is a long chain alcohol that has been seen to enhance homomeric glycine receptor function.

Technology Process of N-DECYL-D21 ALCOHOL

There total 5 articles about N-DECYL-D21 ALCOHOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-decanoic acid (334-48-5) → decanol-d21 (110510-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / NaOD / Pt/C / D₂O / 192 h / 180 °C

2: 6.36 g / LiAlD₄ / tetrahydrofuran / 23 h

With lithium aluminium deuteride; deuteriated sodium hydroxide; platinum on activated charcoal; In tetrahydrofuran; water-d2;

DOI:10.1080/15421400390213311

Reference yield:

d19-decanoic acid (88170-22-3) → decanol-d21 (110510-78-6)

Guidance literature:

With lithium aluminium deuteride; In tetrahydrofuran; for 23h;

DOI:10.1080/15421400390213311

Reference yield:

C5H(2)H7 → decanol-d21 (110510-78-6)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hexamethylsilazane

2: potassium hexamethylsilazane

3: deuterium; palladium on activated charcoal

With palladium on activated charcoal; potassium hexamethylsilazane; deuterium;

upstream raw materials:

d₁₉-decanoic acid

1-decanoic acid

Downstream raw materials:

pentabromophenyl-perdeuterodecyl ether

perdeuterodecyl 4-toluenesulphonylate

Refernces

• 1、 Hughes,Luckhurst,Praefcke,Singer,Tearle. "Chemically-induced discotic liquid crystals. Structural, studies with NMR spectroscopy". . p. 187 - 225. Retrieved 2007/10/03.