18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

Base Information

Chemical Name:18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile
CAS No.:144108-58-7
Molecular Formula:C₄₁H₅₄N₄O₇
Molecular Weight:714.902
Hs Code.:

Synonyms:18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

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Chemical Property of 18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

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Technology Process of 18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

There total 7 articles about 18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1575-61-7
5-Chlorovaleroyl chloride

: 144108-58-7
18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 80 deg C, overnight

3: 81 percent / trifluoroacetic acid / CH₂Cl₂ / 0.25 h / Ambient temperature

4: 100 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

5: 1.) NaH / 1.)DMF, 0 deg C, 30 min, 2.) RT, overnight

With sodium hydroxide; sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00103a012

Reference yield:

: 112139-59-0
O-benzyl-N-(4-cyanobutyl)-hydroxylamine

: 144108-58-7
18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 80 deg C, overnight

3: 81 percent / trifluoroacetic acid / CH₂Cl₂ / 0.25 h / Ambient temperature

4: 100 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

5: 1.) NaH / 1.)DMF, 0 deg C, 30 min, 2.) RT, overnight

With sodium hydroxide; sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00103a012

Reference yield:

: 144108-54-3
N-(benzyloxy)-N-(4-cyanobutyl)-5-chloropentanamide

: 144108-58-7
18-(tert-butoxycarbonyl)-6,12,18-tris(benzyloxy)-7,13-dioxo-6,12,18-triazaoctadecanenitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 80 deg C, overnight

2: 81 percent / trifluoroacetic acid / CH₂Cl₂ / 0.25 h / Ambient temperature

3: 100 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

4: 1.) NaH / 1.)DMF, 0 deg C, 30 min, 2.) RT, overnight

With sodium hydroxide; sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00103a012