25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside

Base Information

• Chemical Name: 25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside
• CAS No.: 168960-81-4
• Molecular Formula: C₅₀H₈₀O₂₃
• Molecular Weight: 1049.17
• Mol file: 168960-81-4.mol

Synonyms:25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside

Chemical Property of 25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside

There total 2 articles about 25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(25R)-26-[(β-D-glucopyranosyl)oxy]-22α-hydroxy-3β-[(β-D-glucopyranosyl-(1→2)-[β-D-xylopyranosyl-(1→3)]-β-D-glucopyranosyl-(1→4)-β-D-galactopyranosyl)oxy]-5α-furostan-12-one → 25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside (168960-81-4)

Guidance literature:

With β-glucosidase; In acetate buffer; at 25 ℃; for 16h; pH=5.0;

DOI:10.1021/np034028a

Reference yield:

hecogenin 3-O-{O-β-D-glucopyranosyl-(1->2)-O-[O-β-D-apiofuranosyl-(1->4)-β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside} → D-apiose (30738-01-3,30912-14-2,36465-64-2,41546-43-4,41546-44-5,41546-45-6,41546-46-7,41546-47-8,41546-48-9,41546-49-0,41546-50-3,63865-04-3,639-97-4,20230-73-3) + 25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside (168960-81-4)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; at 100 ℃; for 2h;

DOI:10.1016/0031-9422(95)00789-X

Reference yield:

25(R)-5α-spirostan-3β-ol-12-one 3-O-β-D-glucopyranosyl-(1->2)-[β-D-xylopyranosyl-(1->3)]-O-β-D-glucopyranosyl-(1->4)-β-D-galactopyranoside (168960-81-4) → hecogenin (467-55-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; for 2h; Heating;

DOI:10.1248/cpb.43.1190

Downstream raw materials:

hecogenin